METHOD FOR TRANSFORMING LEVOGLUCOSENONE INTO 4-HYDROXYMETHYN BUTYROLACTONE OR 4-HYDROXYMETHYL BUTENOLIDE - Archive ouverte HAL Access content directly
Patents Year : 2014

METHOD FOR TRANSFORMING LEVOGLUCOSENONE INTO 4-HYDROXYMETHYN BUTYROLACTONE OR 4-HYDROXYMETHYL BUTENOLIDE

PROCEDE DE TRANSFORMATION DE LEVOGULCOSENONE EN 4-HYDROXYMETHYLBUTYROLACTONE OU 4-HYDROXYMETHYLBUTENOLIDE

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Abstract

The disclosure relates to a method for transforming levoglucosenone into 4-hydroxymethyl butyrolactone or 4-hydroxymethyl butenolide, comprising a step involving the oxidation of the levoglucosenone, or dihydrolevoglucosenone obtained by hydrogenation of levoglucosenone, by bringing a solution of levoglucosenone or dihydrolevoglucosenone in a solvent into contact with a lipase in the presence of an oxidizing agent and an acyl donor compound. The oxidation step is followed by a step involving the hydrolysis of the reaction mixture obtained and, if necessary, a step involving the hydrogenation of the compound obtained at the end of the hydrolysis step.
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Dates and versions

hal-01787823 , version 1 (07-05-2018)

Identifiers

  • HAL Id : hal-01787823 , version 1

Cite

Florent Allais, Amandine Flourat, Aurélien Peru, Andreia Teixeira, Fanny Brunissen, et al.. METHOD FOR TRANSFORMING LEVOGLUCOSENONE INTO 4-HYDROXYMETHYN BUTYROLACTONE OR 4-HYDROXYMETHYL BUTENOLIDE . France, Patent n° : FR20140053957 20140430 / WO2015EP59323 20150429. 2014. ⟨hal-01787823⟩
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