METHOD FOR TRANSFORMING LEVOGLUCOSENONE INTO 4-HYDROXYMETHYN BUTYROLACTONE OR 4-HYDROXYMETHYL BUTENOLIDE

Florent Allais 1, 2 Amandine Flourat 1, 2 Aurélien Peru 1, 2 Andreia Teixeira 1, 2 Fanny Brunissen 1, 2 Henri-Eric Spinnler 3, 2
1 ABI - Agro-Biotechnologies Industrielles
2 AgroParisTech
3 GMPA - Génie et Microbiologie des Procédés Alimentaires
Abstract : The disclosure relates to a method for transforming levoglucosenone into 4-hydroxymethyl butyrolactone or 4-hydroxymethyl butenolide, comprising a step involving the oxidation of the levoglucosenone, or dihydrolevoglucosenone obtained by hydrogenation of levoglucosenone, by bringing a solution of levoglucosenone or dihydrolevoglucosenone in a solvent into contact with a lipase in the presence of an oxidizing agent and an acyl donor compound. The oxidation step is followed by a step involving the hydrolysis of the reaction mixture obtained and, if necessary, a step involving the hydrogenation of the compound obtained at the end of the hydrolysis step.
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Patents
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https://hal-agroparistech.archives-ouvertes.fr/hal-01787823
Contributor : Grégoire Burgé <>
Submitted on : Monday, May 7, 2018 - 6:12:46 PM
Last modification on : Wednesday, July 3, 2019 - 11:22:09 AM

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  • HAL Id : hal-01787823, version 1

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AGROPARISTECH | INRA

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Florent Allais, Amandine Flourat, Aurélien Peru, Andreia Teixeira, Fanny Brunissen, et al.. METHOD FOR TRANSFORMING LEVOGLUCOSENONE INTO 4-HYDROXYMETHYN BUTYROLACTONE OR 4-HYDROXYMETHYL BUTENOLIDE . France, Patent n° : FR20140053957 20140430 / WO2015EP59323 20150429. 2014. ⟨hal-01787823⟩

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